WebNov 4, 2014 · The excess of the T3P ® reagent was hydrolyzed with 10% NaHCO 3 solution (15 mL) and the aqueous phase was washed with ethyl acetate (30 mL). The combined organic phase was dried (Na 2 SO 4 ), and concentrated in vacuum to provide the crude product that was passed through a thin (ca. 3–4 cm) layer of silica gel using 3% MeOH in … WebPropylphosphonic anhydride solution ≥50 wt. % in ethyl acetate Synonym (s): 1-Propanephosphonic anhydride solution, 2,4,6-Tripropyl-1,3,5,2,4,6-trioxatriphosphorinane-2,4,6-trioxide solution, PPACA, T3P® Empirical Formula (Hill Notation): C9H21O6P3 CAS Number: 68957-94-8 Molecular Weight: 318.18 Beilstein: 5079255 MDL number: …

A solvent-reagent selection guide for Steglich-type esterification …

Webthe synthesis of amides. 8 T3P® is a mild reagent that is avail-able in ethyl acetate solution and is easy to handle. It has useful properties such as broad functional group tolerance and low toxicity, and its use results in simple work-up pro-cedures.9 For these reasons, new applications have been re- Web(50% solution in ethyl acetate) for synthesis T3P Synonym (s): 2,4,6-Tripropyl-1,3,5,2,4,6-trioxatriphosphorinane-2,4,6-trioxide solution, PPACA, Propylphosphonic anhydride, T3P … team inc heat treat

Amide synthesis by acylation - Organic Chemistry

WebMay 25, 2024 · Novel and convenient methodology for the construction of N-substituted amide derivatives have been developed from nitriles and alcohols using propylphosphonic anhydride (T3P ®). This methodology is an alternate approach to the synthesis of amides via Ritter reaction, which is one of the classical methods for the synthesis of N … WebT3P (50% solution ethyl acetate) This product is a chemical and requires you to have an SLS credit account. WebDate HS Code Description Origin Country Port of Discharge Unit Quantity Value (INR) Per Unit (INR) Oct 21 2016: 29420090: PROPYLPHOSPHONIC ANHYDRIDE (T3P), 50% WH.IN ETHYL ACETATE AGN-PC-0JLL6O sov thermostat